1-(4-氯苯基)-1,2-丙二酮合成路线 (共 14 条)
反应条件
pyridinium chlorochromate in dichloromethane T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Bhosale, Shrikar M.; Momin, Aadil A.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5327 - 5330
反应条件
air; 4-aminoperbenzoic acid in dichloromethane T=20°C; 12 h;
参考文献
Ghazanfari, Dadkhoda; Najafizadeh, Fariba; Khosravi, Fereshteh
Monatshefte fur Chemie, 2004 , vol. 135, # 11 p. 1409 - 1413
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran; dimethyl sulfoxide T=20°C; 3 h;
参考文献
Yadav; Biswas, Swapan Kumar; Srinivas
Synthesis, 2006 , # 24 p. 4237 - 4241
反应条件
2,2'-azo-bisisobutyronitrile; oxygen; palladium diacetate; sodium carbonate T=120°C; P=6080.41 Torr; 20 h; Autoclave;
参考文献
Wang, Azhong; Jiang, Huanfeng; Li, Xianwei
Journal of Organic Chemistry, 2011 , vol. 76, # 16 p. 6958 - 6961
反应条件
potassium permanganate; magnesium sulfate in toluene T=50 - 60°C; 40 h;
参考文献
Aitken, R. Alan; Cadogan, J. I. G.; Gosney, Ian
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 101, # 1-4 p. 281 - 286
反应条件
sulfuric acid Heating;
参考文献
Bratchanskii, P. E.; Komissarova, G. G.; Esipov, G. V.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 10 p. 1961 - 1964
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 10 p. 2143 - 2147
反应条件
cobalt(II) chloride in acetonitrile 24 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , p. 692 - 693
反应条件
selenium(IV) oxide in ethanol 48 h; Heating;
参考文献
Bulletin de la Societe Chimique de France, , p. 1921 - 1925
反应条件
hydrogenchloride; formaldehyd T=20°C;
参考文献
Russian Chemical Bulletin, , vol. 55, # 6 p. 1046 - 1051
反应条件
1: sulfur / benzene / 1 h / 25 - 60 °C 2: dilute hydrochloric acid View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 10 p. 1961 - 1964
Zhurnal Organicheskoi Khimii, , vol. 21, # 10 p. 2143 - 2147