4-(4-氯苯甲酰基)苯甲醚合成路线 （共 37 条）
反应条件
copper ferrite in 1,2-dichloro-ethane T=35 - 38°C; Friedel-Crafts Acylation; 18 h;
参考文献
Parella, Ramarao; Naveen; Kumar, Amit; Babu, Srinivasarao Arulananda
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1738 - 1742
反应条件
1: 1-bromo-4-methoxy-benzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: 4-chlorobenzaldehyde in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; 3: With iodine; potassium carbonate in tert-butyl alcohol 3 h; Reflux;
参考文献
Ushijima, Sousuke; Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 5 p. 1436 - 1442
反应条件
1: 1-chloro-4-bromobenzene With magnesium in tetrahydrofuran T=20°C; 1 h; 2: 4-methoxy-benzaldehyde in tetrahydrofuran T=0 - 20°C; 2 h; 3: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrahydrofuran; tert-butyl alcohol 20 h; RefluxDarkness;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 32 p. 6557 - 6564
反应条件
1: With methyltrichloromonosilane; anhydrous iron chloride T=20 - 40°C; 24 h; 2: With ethanol in chlorobenzene T=0°C;
参考文献
Shasun Pharma Solutions Limited
Patent: US2008/154049 A1, 2008 ;
Location in patent: Page/Page column 13 ;
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
反应条件
potassium carbonate in methoxybenzene T=80°C; carbonylative Suzuki-Miyaura cross-coupling; P=760.051 Torr; 8 h;
参考文献
Cai, Mingzhong; Peng, Jian; Hao, Wenyan; Ding, Guodong
Green Chemistry, 2011 , vol. 13, # 1 p. 190 - 196
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=0°C;
参考文献
Duplais, Christophe; Bures, Filip; Sapountzis, Ioannis; Korn, Tobias J.; Cahiez, Gerard; Knochel, Paul
Angewandte Chemie - International Edition, 2004 , vol. 43, # 22 p. 2968 - 2970
反应条件
sodium lauryl sulfate; potassium carbonate; palladium dichloride in water T=60°C; 6 h;
参考文献
Xin, Bingwei; Zhang, Yuhong; Cheng, Kai
Synthesis, 2007 , # 13 p. 1970 - 1978
反应条件
sodium lauryl sulfate; potassium carbonate; palladium dichloride in water T=60°C; 6 h;
参考文献
Xin, Bingwei; Zhang, Yuhong; Cheng, Kai
Synthesis, 2007 , # 13 p. 1970 - 1978
反应条件
1: With N-iodo-succinimide; N-hexadecyl-N,N,N-trimethylammonium bromide; acetic acid in 1,4-dioxane; water T=20°C; 2: in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation; 3: With tert.-butylhydroperoxide; dipyridinium dichromate in 1,4-dioxane; water T=115°C; 0.25 h; Microwave irradiation;
参考文献
Sharma, Naina; Sharma, Abhishek; Kumar, Rakesh; Shard, Amit; Sinha, Arun K.
European Journal of Organic Chemistry, 2010 , # 31 p. 6025 - 6032
