2,6-二溴-4-叔丁基苯胺合成路线 （共 6 条）
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide 2 h; Ambient temperature;
参考文献
Miura; Oka; Momoki
Synthesis, 1995 , # 11 p. 1419 - 1422
反应条件
hydrogen bromide; dihydrogen peroxide in water T=20°C; 24 h; Darkness;
参考文献
Podgorsek, Ajda; Stavber, Stojan; Zupan, Marko; Iskra, Jernej
Tetrahedron, 2009 , vol. 65, # 22 p. 4429 - 4439
反应条件
bromine; acetic acid
参考文献
Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1602,1603
反应条件
1.1: sodium nitrite; sulfuric acid / acetic acid / 4 h / 20 °C 1.2: 20 °C 2.1: n-butyllithium / hexane; diethyl ether / 2 h / -78 °C 2.2: 1 h / -78 °C 2.3: 12 h / 20 °C View Scheme
参考文献
Guo, Zhengqing; Yiu, Shek-Man; Chan, Michael C. W.
Chemistry - A European Journal, 2013 , vol. 19, # 27 p. 8937 - 8947
反应条件
sulfuric acid; sodium nitrite in ethanol T=50 - 80°C;
参考文献
Hu, Wen-Jing; Zhao, Xiao-Li; Ma, Ming-Liang; Guo, Fang; Mi, Xian-Qiang; Jiang, Biao; Wen, Ke
European Journal of Organic Chemistry, 2012 , # 7 p. 1448 - 1454
反应条件
pyridine
Erwaermen des Reaktionsprodukts mit wss. Natronlauge;
参考文献
Drake et al.
Journal of the American Chemical Society, 1946 , vol. 68, p. 1602,1603
