(3-溴丙基)(三甲基)硅烷合成路线 （共 26 条）
反应条件
1: 73 percent
2: m-cloroperbenzoic acid
3: 1.) n-BuLi-TMEDA / 1.) THF, -70-0 deg C, 1 h; 2.) 0 deg C, 9 h
View Scheme
参考文献
Hosomi, Akira; Inaba, Masahiro; Sakurai, Hideki
Chemistry Letters, 1983 , p. 1763 - 1766
反应条件
1: 73 percent
2: m-cloroperbenzoic acid
3: 1.) n-BuLi-TMEDA / 1.) THF, -70-0 deg C, 1 h; 2.) 0 deg C, 8 h
View Scheme
参考文献
Hosomi, Akira; Inaba, Masahiro; Sakurai, Hideki
Chemistry Letters, 1983 , p. 1763 - 1766
反应条件
1: 73 percent
2: m-cloroperbenzoic acid
3: 1.) n-BuLi-TMEDA / 1.) THF, -70-0 deg C, 1 h; 2.) 0 deg C, 14 h
View Scheme
参考文献
Hosomi, Akira; Inaba, Masahiro; Sakurai, Hideki
Chemistry Letters, 1983 , p. 1763 - 1766
反应条件
1: 73 percent
2: 1.) t-BuLi-HMPA / 1.) THF, pentane, -78 deg C, 2 h; 2.) -20 deg C, 5 h
View Scheme
参考文献
Hosomi, Akira; Inaba, Masahiro; Sakurai, Hideki
Chemistry Letters, 1983 , p. 1763 - 1766
反应条件
1: 73 percent
2: 1.) t-BuLi-HMPA / 1.) THF, pentane, -78 deg C, 2 h; 2.) -20 deg C, 5 h
View Scheme
参考文献
Hosomi, Akira; Inaba, Masahiro; Sakurai, Hideki
Chemistry Letters, 1983 , p. 1763 - 1766
反应条件
1: 73 percent
2: 1.) t-BuLi-HMPA / 1.) THF, pentane, -78 deg C, 2 h; 2.) -20 deg C, 5 h
View Scheme
参考文献
Hosomi, Akira; Inaba, Masahiro; Sakurai, Hideki
Chemistry Letters, 1983 , p. 1763 - 1766
