4-(甲基氨基)苯甲酸乙酯合成路线 （共 22 条）
反应条件
1: With potassium salt of diphenylphosphine anion in tetrahydrofuran T=-78°C; 2 h; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water Inert atmosphere;
参考文献
Yoshida, Suguru; Igawa, Kazunobu; Tomooka, Katsuhiko
Journal of the American Chemical Society, 2012 , vol. 134, # 47 p. 19358 - 19361
反应条件
N-ethyl-N,N-diisopropylamine T=95 - 120°C; 1 h;
参考文献
EP2033949 A1, ;
Page/Page column 31 ;
反应条件
potassium phosphate; [Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos) in 1,4-dioxane; tert-butyl alcohol T=110°C; Buchwald-Hartwig Coupling; Inert atmosphereGlovebox; chemoselective reaction;
参考文献
Alsabeh, Pamela G.; Stradiotto, Mark
Angewandte Chemie - International Edition, 2013 , vol. 52, # 28 p. 7242 - 7246
Angew. Chem., 2013 , vol. 125, # 28 p. 7383 - 7387
反应条件
potassium carbonate in acetonitrile T=80°C; 6 h;
参考文献
Organic Letters, , vol. 11, # 6 p. 1225 - 1228
反应条件
1: 33 percent / 1-(p-tolyl)-1-methylhydrazine, PbO2 2: 1,2-dimethoxy-ethane / 1 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 22 p. 4448 - 4455
反应条件
Na(OAc)BH3 in tetrahydrofuran T=20°C; 3 h;
参考文献
Tetrahedron, , vol. 66, # 35 p. 7142 - 7148
反应条件
sodium cyanoborohydride; acetic acid in tetrahydrofuran; water T=20°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 18, # 14 p. 4022 - 4026
反应条件
1: 33 percent / 1-<p-(ethoxycarbonyl)phenyl>-1-methylhydrazine, PbO2 2: 1,2-dimethoxy-ethane / 1 h / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 22 p. 4448 - 4455
反应条件
sodium hydroxide 1 h; Heating;
参考文献
Briggs, Elizabeth; Brown, Geoffrey W.; Jiricny, Josef; Meidine, Mohamed F.
Synthesis, 1980 , # 4 p. 295 - 296
反应条件
dimethylsulfide borane complex in tetrahydrofuran 2 h; Heating; Yield given;
参考文献
Tetrahedron Letters, , vol. 23, # 33 p. 3315 - 3318
