2-甲氧基-N-甲基苯胺合成路线 (共 36 条)
反应条件
sodium tetrahydroborate; sodium methylate in methanol 1) room temp., 5 h, 2) reflux;
参考文献
Barluenga, Jose; Bayon, Ana M.; Asensio, Gregorio
Journal of the Chemical Society, Chemical Communications, 1984 , # 20 p. 1334 - 1335
反应条件
lithium aluminium tetrahydride; ammonium chloride in tetrahydrofuran; formic acid ethyl ester
参考文献
US6245799 B1, ;
US 6245799 B1
反应条件
pyridine; copper diacetate in 1,4-dioxane Chan-Lam reaction; 3 h; Reflux;
参考文献
Gonzalez, Israel; Mosquera, Jesus; Guerrero, Cesar; Rodriguez, Ramon; Cruces, Jacobo
Organic Letters, 2009 , vol. 11, # 8 p. 1677 - 1680
反应条件
copper in water T=100°C; Ullmann reaction; 16 h;
参考文献
Jiao, Jiao; Zhang, Xi-Ru; Chang, Ning-Hui; Wang, Jie; Wei, Jun-Fa; Shi, Xian-Ying; Chen, Zhan-Guo
Journal of Organic Chemistry, 2011 , vol. 76, # 4 p. 1180 - 1183
反应条件
copper in water T=100°C; Ullmann reaction; 16 h;
参考文献
Jiao, Jiao; Zhang, Xi-Ru; Chang, Ning-Hui; Wang, Jie; Wei, Jun-Fa; Shi, Xian-Ying; Chen, Zhan-Guo
Journal of Organic Chemistry, 2011 , vol. 76, # 4 p. 1180 - 1183
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=20°C; 0.5 h;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 22 p. 2520 - 2524
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 12 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 76, # 5 p. 1063 - 1070
反应条件
1: With tin(IV) chloride T=20°C; 2: With lithium aluminium tetrahydride in tetrahydrofuran 24 h; Heating;
参考文献
Chemistry Letters, , vol. 32, # 6 p. 548 - 549
反应条件
phosphorus; hydrogen iodide T=100°C;
参考文献
Chemische Berichte, , vol. 49, p. 581
Journal of the Chemical Society, , vol. 101, p. 548
Archiv der Pharmazie (Weinheim, Germany), , vol. 246, p. 15,21
反应条件
phosphorus; hydrogen iodide T=100°C;
参考文献
Chemische Berichte, , vol. 49, p. 581
Journal of the Chemical Society, , vol. 101, p. 548
Archiv der Pharmazie (Weinheim, Germany), , vol. 246, p. 15,21