N,N’,N”-三甲基二乙烯三胺合成路线 (共 7 条)
反应条件
caesium carbonate; thiophenol in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
TIBOTEC PHARMACEUTICALS; VENDEVILLE, Sandrine, Marie, Helene; RABOISSON, Pierre, Jean-Marie, Bernard; LIN, Tse-I
Patent: WO2010/3658 A1, 2010 ;
Location in patent: Page/Page column 47-48 ;
反应条件
lithium aluminium tetrahydride in ethylene glycol dimethyl ether Heating;
参考文献
Tuladhar; D'Silva
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2203 - 2206
反应条件
in water T=20°C; 336000 h;
参考文献
Tetrahedron, , vol. 59, # 38 p. 7565 - 7570
反应条件
1: dimethylformamide / 1 h / 110 °C 2: 66 percent / 96percent aq. H2SO4 / 72 h / 100 °C View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 7 p. 1059 - 1065
参考文献
Journal of Polymer Science, , vol. 40, p. 343,345
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US5583256 A1, 1996 ;
反应条件
(i) ClCO2Et, Et3N, (ii) /BRN= 1736861/; Multistep reaction;
参考文献
Bayer AG
Patent: DE2515146 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 71947