(3-乙酰氧基-2-羟基丙基)乙酸酯合成路线 (共 34 条)
反应条件
triethylamine in dichloromethane
参考文献
Fujisawa Pharmaceutical Co., Ltd.
Patent: US6884868 B1, 2005 ;
US 6884868 B1
参考文献
Engel
Journal of the American Chemical Society, 1953 , vol. 57, p. 2423
参考文献
Engel
Journal of the American Chemical Society, 1953 , vol. 57, p. 2423
反应条件
1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 80 °C
2.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C
2.2: 3 h / -78 °C
View Scheme
参考文献
Sari, Ozkan; Hamada, Manabu; Roy, Vincent; Nolan, Steven P.; Agrofoglio, Luigi A.
Organic Letters, 2013 , vol. 15, # 17 p. 4390 - 4393