N-(4-氯苄基)-1-(4-乙炔苯基)甲胺合成路线 (共 3 条)
反应条件
1: in methanol T=20°C; 16 h; 2: With sodium tetrahydroborate in methanol Product distribution / selectivity;
参考文献
Deng, Xiaoliu; Liang, Jimmy T.; Peterson, Matthew; Rynberg, Raymond; Cheung, Eugene; Mani, Neelakandha S.
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 1940 - 1947
反应条件
1: With acetic acid in dichloromethane 0.5 h; 2: With sodium tris(acetoxy)borohydride in dichloromethane 72 h; Product distribution / selectivity;
参考文献
Ameriks, Michael K.; Axe, Frank U.; Edwards, James P.; Grice, Cheryl A.; Cai, Hui; Gleason, Elizabeth Ann; Meduna, Steven P.; Tays, Kevin L.; Wiener, John J. M.; Wickboldt, Alvah T.
Patent: US2008/200454 A1, 2008 ;
Location in patent: Page/Page column 73 ;
US 20080200454 A1
反应条件
sodium tris(acetoxy)borohydride; acetic acid in dichloromethane
参考文献
Deng, Xiaoliu; Liang, Jimmy T.; Peterson, Matthew; Rynberg, Raymond; Cheung, Eugene; Mani, Neelakandha S.
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 1940 - 1947