2-氧代环戊烷羧酸甲酯合成路线 （共 119 条）
反应条件
(i) NaBH4, (ii) P2O5; Multistep reaction;
参考文献
Rhoads,S.J. et al.
Journal of Organic Chemistry, 1970 , vol. 35, # 10 p. 3352 - 3358
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Dreiding; Hartman
Journal of the American Chemical Society, 1953 , vol. 75, p. 939,940
反应条件
2: 97 percent / KOH / methanol; H2O / 15 h / Heating View Scheme
参考文献
Neudeck, Horst K.
Monatshefte fuer Chemie, 1989 , vol. 120, p. 597 - 622
反应条件
sea sand; sodium ethanolate; potassium hexacyanoferrate(III) 1.) RT, 10 min, 2.) RT, 3 h; Yield given. Multistep reaction;
参考文献
Kornblum, Nathan; Kelly, William J.; Kestner, M. M.
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4720 - 4724
反应条件
1: 86 percent / NaH / dimethylformamide / 2 h / 100 °C 2: 35 percent / NaCl, H2O / dimethylsulfoxide / 3 h / 180 °C 3: sulfuryl chloride / CCl4 / 24 h / Ambient temperature 4: γ-collidine View Scheme
参考文献
Yamane, Hisakazu; Sugawara, Jun; Suzuki, Yasushi; Shimamura, Etsuko; Takahashi, Nobutaka
Agricultural and Biological Chemistry, 1980 , vol. 44, # 12 p. 2857 - 2864
反应条件
hydrogenchloride; sodium nitrite in tetrahydrofuran; potassium hydroxide; water; benzene
参考文献
Warner-Lambert Company
Patent: US5284862 A1, 1994 ;
反应条件
triethylammonium phosphinate; tris(triphenylphosphine)ruthenium(II) chloride in methanol T=40°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Khai, Bui The; Arcelli, Antonio
Tetrahedron Letters, 1996 , vol. 37, # 36 p. 6599 - 6602
反应条件
water T=200°C; im Rohr;
参考文献
Meerwein
Justus Liebigs Annalen der Chemie, 1913 , vol. 398, p. 249
反应条件
T=200°C; im geschlossenen Rohr;
参考文献
Meerwein
Justus Liebigs Annalen der Chemie, 1913 , vol. 398, p. 249
反应条件
4-(N,N-dimethlyamino)pyridine in toluene 12 h; Heating;
参考文献
Schultz, Arthur G.; Holoboski, Mark A.
Tetrahedron Letters, 1993 , vol. 34, # 19 p. 3021 - 3024
