2-氧代环戊烷羧酸甲酯合成路线 (共 119 条)
反应条件
sodium hydride in toluene 5 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 45, # 14 p. 2766 - 2772
反应条件
1) 650 deg C, 10-4 mbar, 2) CCl4; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 57, # 18 p. 4850 - 4858
反应条件
(i) (irradiation), Et2O, (ii) /BRN= 102415/; Multistep reaction;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 12, p. 1251 - 1260,1252 - 1260
反应条件
(i) NaNH2, nPr2O, (ii) /BRN= 635994/; Multistep reaction;
参考文献
Chemische Berichte, , vol. 93, p. 1212 - 1219
参考文献
Chemische Berichte, , vol. 89, p. 60,65
反应条件
1: K2CO3 / acetone / Heating 2: 2.6 g / glacial AcOH; 6M HCl / Heating View Scheme
参考文献
Pearson, William H.; Walavalkar, Rajesh; Schkeryantz, Jeffrey M.; Fang, Wen-Kui; Blickensdorf, James D.
Journal of the American Chemical Society, 1993 , vol. 115, # 22 p. 10183 - 10194
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; sodium hydride in tetrahydrofuran T=80°C; 10 h; Heating;
参考文献
Dowd, Paul; Choi, Soo-Chang
Journal of the American Chemical Society, 1987 , vol. 109, # 11 p. 3493 - 3494
反应条件
1: 58 percent / sodium hydride / 1.) THF, 0 deg C, 1 h, 2.) reflux, 12 h 2: 75 percent / 6M HCl / 36 h / Heating 3: 1.) TEOF, 2.) potassium tert-butoxide / 1.) CH2Cl2, 12h, 2.) THF, 0 deg C View Scheme
参考文献
Garst, M. E.; Johnson, A. T.
Tetrahedron Letters, 1980 , vol. 21, p. 4811 - 4814
反应条件
in ethanol T=60°C; 0.5 h;
参考文献
Bagrov, F. V.; Molchadskii, A. S.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 1.1 p. 72 - 75
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 1 p. 87 - 91
反应条件
1: 86 percent / NaH / dimethylformamide / 2 h / 100 °C 2: 35 percent / NaCl, H2O / dimethylsulfoxide / 3 h / 180 °C View Scheme
参考文献
Yamane, Hisakazu; Sugawara, Jun; Suzuki, Yasushi; Shimamura, Etsuko; Takahashi, Nobutaka
Agricultural and Biological Chemistry, 1980 , vol. 44, # 12 p. 2857 - 2864