2-(4,5-二氢呋喃-2-基)-4,4,5,5-四甲基-1,3,2-二氧杂硼烷 4,5-二氢-5-呋喃基硼酸频哪醇酯合成路线 (共 2 条)
反应条件
4,4'-di-tert-butyl-2,2'-dipyridyl; bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I) in octane T=80°C; 8 h; Title compound not separated from byproducts.;
参考文献
Chemistry Letters, , vol. 37, # 6 p. 664 - 665
反应条件
catalyst:(Ir(COD)OCH3)2/2(4,4'-di-tert-butyl-bipy) in hexane heating in hexane at 25-80°C in the presence of (Ir(OMe)(COD))2/2(4,4'-di-tert-butyl-bipy); (.alpha/β=49/51);
参考文献
Bulletin of the Chemical Society of Japan, , vol. 81, # 12 p. 1535 - 1553