5-甲基-2-异丙基环己酮合成路线 （共 238 条）
反应条件
Multi-step reaction with 4 steps 4: 80 percent / NaIO4 / methanol / -5 °C
参考文献
Menon; Kumar; Ravindranathan Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5313 - 5314
反应条件
Multi-step reaction with 5 steps 4: 80 percent / NaIO4 / methanol / -5 °C5: LDA, TMEDA / tetrahydrofuran
参考文献
Menon; Kumar; Ravindranathan Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5313 - 5314
反应条件
With hydrogenchloride in Petroleum ether
参考文献
Menon; Kumar; Ravindranathan Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5313 - 5314
参考文献
Menon; Kumar; Ravindranathan Tetrahedron Letters, 1987 , vol. 28, # 44 p. 5313 - 5314
反应条件
Multi-step reaction with 3 steps 1: hydroxylamine hydrochloride; sodium carbonate / ethanol; water / 120 h / 25 °C2: sulfuric acid; N,N,N,N',N',N'-hexamethyl-butane-1,4-diammonium dimethylsulfate / methanol; water / 50 °C / Electrochemical reduction3: triethylamine / dichloromethane / 0 - 20 °C
参考文献
Kulisch, Joern; Nieger, Martin; Stecker, Florian; Fischer, Andreas; Waldvogel, Siegfried R. Angewandte Chemie - International Edition, 2011 , vol. 50, # 24 p. 5564 - 5567
反应条件
With trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-40°C; Yield given;
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Oku, Akira Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4843 - 4846
反应条件
Multi-step reaction with 2 steps 1: 1) LDA / 1) THF, -80 deg C2: TfOH / tetrahydrofuran / 2 h / -40 °C
参考文献
Harada, Toshiro; Tanaka, Sachi; Oku, Akira Tetrahedron, 1992 , vol. 48, # 40 p. 8621 - 8630
反应条件
With trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-40°C; Yield given;
参考文献
Harada, Toshiro; Kurokawa, Hideaki; Oku, Akira Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4843 - 4846
