5-甲基-2-异丙基环己酮合成路线 （共 238 条）
反应条件
[bis(acetoxy)iodo]benzene in water; acetonitrile T=20°C; Ring cleavage; 0.0333333 h;
参考文献
Shi; Wu
Synthetic Communications, 2000 , vol. 30, # 22 p. 4081 - 4086
反应条件
water; fluorine; acetonitrile in chloroform T=-10 - 0°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 49, # 36 p. 8169 - 8178
反应条件
[Ru(PnOct3)4(H)2] in o-xylene 24 h; Inert atmosphereRefluxGloveboxSchlenk technique; Time;
参考文献
US2014/73817 A1, ;
Paragraph 0097 ;
反应条件
HOF* CH3CN; NAF in chloroform; water; acetonitrile 0 deg C -> room temperature;
参考文献
Journal of Organic Chemistry, , vol. 60, # 25 p. 8267 - 8269
反应条件
[Ru(PnOct3)4(H)2] in o-xylene 12 h; Inert atmosphereHeatingGloveboxAutoclaveSchlenk technique; Reagent/catalyst;
参考文献
US2014/73817 A1, ;
Paragraph 0094 ;
反应条件
toluene-4-sulfonic acid 15 h; Ambient temperature;
参考文献
Harada, Toshiro; Inoue, Atsushi; Wada, Isao; Uchimura, Jun-Ji; Tanaka, Sachi; Oku, Akira
Journal of the American Chemical Society, 1993 , vol. 115, # 17 p. 7665 - 7674
反应条件
((n-Bu)4N)2S2O8 in 1,2-dichloro-ethane 2 h; Heating;
参考文献
Chen, Fener; Liu, Anchang; Yan, Qiongjiao; Liu, Mingxing; Zhang, Daoming; Shao, Lanying
Synthetic Communications, 1999 , vol. 29, # 6 p. 1049 - 1056
反应条件
dipyridinium dichromate; chloro-trimethyl-silane in dichloromethane 1 h;
参考文献
Cossio, Fernando P.; Aizpurua, Jesus M.; Palomo, Claudio
Canadian Journal of Chemistry, 1986 , vol. 64, p. 225 - 231
反应条件
1: 89 percent / KH / tetrahydrofuran / 3.5 h / Ambient temperature 2: p-toluenesulfonic acid / 15 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 17 p. 7665 - 7674
反应条件
1: 84 percent / KH / tetrahydrofuran / 3.5 h / Ambient temperature 2: conc. aq. HCl / methanol / 22 h / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 115, # 17 p. 7665 - 7674
