titanium tetra-n-butoxide
2.5 h; Heatingother catalysts other reaction time degree of esterification estimated by titration with KOH; Title compound not separated from byproducts;
参考文献
Novrocik, Jan; Novrocikova, Marta; Norek, Jiri; Koruna, Ivan; Ryska, Miroslav
Collection of Czechoslovak Chemical Communications, 1984 , vol. 49, # 1 p. 253 - 266
in further solvent(s)
addn. of C6H8O4Sn to C4H9CH(C2H5)CH2OH, suspn. mixed thoroughly, dropwise addn. of concd. HCl until C6H8O4Sn was consumed, water and alcohol removed by heating; purifn. by vac. distn.; elem. anal., mass spectroscopy;
参考文献
Cheng, Hong-Shing; Hwang, Tsai-Lih; Liu, Chao-Shiuan
Journal of Organometallic Chemistry, 1983 , vol. 254, # 1 p. 43 - 52