hydrogenchloride; titanium(III) chloride; aluminium in ethanol T=20°C; pinacol coupling; 0.833333 h; sonication; Title compound not separated from byproducts;
1: With [CpFe(CO)2(PCy3)][BF4]; phenyl silane T=100°C; IrradiationNeat (no solvent)Inert atmosphere; 2: With hydrogenchloride; water in tetrahydrofuran T=20°C; 1 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 10 p. 1879 - 1884
