4-(4-甲氧苯基)-2-丁酮合成路线 (共 82 条)
反应条件
1: 38 percent / TMEDA; Zn / TiCl4 / CH2Cl2; tetrahydrofuran 2: 78 percent / B(C6F5)3 / CH2Cl2 / 0.08 h / 20 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 345, # 8 p. 1017 - 1030
反应条件
hydrogen T=75°C; P=3750.38 Torr; 1.25 h;
参考文献
Green Chemistry, , vol. 12, # 1 p. 99 - 107
反应条件
1: aq. NaOH 2: 90 percent / H2 / Pd/C / ethanol / 20 °C / 3102.89 Torr View Scheme
参考文献
Journal of Organic Chemistry, , vol. 63, # 9 p. 2867 - 2872
反应条件
in water; acetonitrile 0.416667 h; UV-irradiation;
参考文献
Wang, Pengfei; Wang, Yun; Hu, Huayou; Spencer, Cierra; Liang, Xing; Pan, Lurong
Journal of Organic Chemistry, 2008 , vol. 73, # 16 p. 6152 - 6157
反应条件
acetone; palladium dichloride Hydrogenation;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 439, p. 303
反应条件
1.1: 91 percent / tetrahydrofuran / -78 °C 2.1: n-BuLi / tetrahydrofuran; hexane / -15 °C 2.2: tetrahydrofuran; hexane / -78 - 20 °C 2.3: 79 percent / aq. HCl / tetrahydrofuran; hexane; diethyl ether / 20 °C View Scheme
参考文献
Organic Letters, , vol. 7, # 7 p. 1427 - 1429
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate 1 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 31, # 1 p. 60 - 62
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate 1 h;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 31, # 1 p. 60 - 62
反应条件
RhCl3(H2O)3; (+/-)2,2'-bis(diphenylphosphino)-1,1'-binaphthalene in water; toluene T=80°C; 40 h; Heating;
参考文献
Zou, Gang; Guo, Jianping; Wang, Zhiyong; Huang, Wen; Tang, Jie
Dalton Transactions, 2007 , # 28 p. 3055 - 3064
反应条件
sodium acetate; palladium diacetate in acetonitrile T=60°C; 0.333333 h; Product distribution; Further Variations:ReagentsCatalystsSolventstime;
参考文献
Synthesis, , # 20 p. 3443 - 3452