(9ci)-5-氯-1-甲基-1H-苯并咪唑合成路线 (共 7 条)
反应条件
1: 6-chloro-1H-benzo[d]imidazole With sodium hydride in tetrahydrofuran T=0°C; 0.25 h; 2: methyl iodide in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Nakao, Yoshiaki; Kanyiva, Kyalo Stephen; Oda, Shinichi; Hiyama, Tamejiro
Journal of the American Chemical Society, 2006 , vol. 128, # 25 p. 8146 - 8147
反应条件
potassium hydrogensulfate; sodium sulfate 24 h; mortar;
参考文献
Zefirov; Sereda; Volkov; Tkachenko; Zyk
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 5 p. 577 - 579
反应条件
1: H2SO4; NaNO2 2: tin; hydrochloric acid View Scheme
参考文献
Pinnow
Chemische Berichte, 1898 , vol. 31, p. 2984
反应条件
hydrogenchloride; tin
参考文献
Pinnow
Chemische Berichte, 1898 , vol. 31, p. 2984
参考文献
Aliprandi et al.
Annali di Chimica (Rome, Italy), 1958 , vol. 48, p. 1349,1354
参考文献
Davies et al.
Journal of Pharmacy and Pharmacology, 1951 , vol. 3, p. 420,424
Full Text Show Details
Feitelson et al.
Journal of the Chemical Society, 1952 , p. 2389,2393
参考文献
Pinnow
Chemische Berichte, 1898 , vol. 31, p. 2984