反应条件
1: 1) BuLi / THF, -78 deg C
2: Bu4NF / tetrahydrofuran / Ambient temperature
3: pyridine / Ambient temperature
4: aq. HCl / Ambient temperature
5: DMAP, pyridine / 100 °C
6: 93 percent / H2SO4 / acetic acid / Ambient temperature
7: 95 percent / trimethylsilyl triflate / acetonitrile / 0 - 20 °C
8: 85 percent / NH3 / methanol / Ambient temperature
View Scheme
参考文献
Matsuda, Akira; Hattori, Hideshi; Tanaka, Motohiro; Sasaki, Takuma
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 16 p. 1887 - 1892
