1: With tetrabutylammonium trifluoromethanesulphonate in acetonitrile T=20°C; 8 h; Electrochemical reactionUndivided electrochemical cell with aluminum anode/platinum cathodeInert atmosphere; 2: With hydrogenchloride; water in acetonitrile Inert atmosphere;
phosphorus trichoride; dilithium tetrachlorocuprate in tetrahydrofuran
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 3.2 p. 635
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 3 p. 714 - 715