反应条件
1: 2,4,6-triphenyl-1-bromobenzene With n-butyllithium in diethyl ether; hexane
T=20°C; 2 h;
2: 2,4,6-triphenyl-1-bromobenzene in diethyl ether; hexane
T=-78 - 20°C;
3: With lithium aluminium tetrahydride in diethyl ether; hexane
T=20°C; 2.5 h; Further stages.;
参考文献
Blank, Natalia F.; Moncarz, Jillian R.; Brunker, Tim J.; Scriban, Corina; Anderson, Brian J.; Amir, Omar; Glueck, David S.; Zakharov, Lev N.; Golen, James A.; Incarvito, Christopher D.; Rheingold, Arnold L.
Journal of the American Chemical Society, 2007 , vol. 129, # 21 p. 6847 - 6858