反应条件
1: hexane carboxylic acid With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane
T=-78 - -35°C; 1 h; Inert atmosphere;
2: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical With Fe(η5-C5H5)2(PF6) in tetrahydrofuran; hexane
T=-78°C; 0.5 h; Inert atmosphere;
参考文献
Dinca, Emanuela; Hartmann, Philip; Smrcek, Jakub; Dix, Ina; Jones, Peter G.; Jahn, Ullrich
European Journal of Organic Chemistry, 2012 , # 24 p. 4461 - 4482