4,5-二氢-2-[(3-甲基-2-丁烯-1-基)硫基]噻唑合成路线 （共 2 条）
反应条件
sodium hydride in N,N-dimethyl-formamide T=10°C; 1.) 15 min, 2.) 15 min;
参考文献
Veselovskii, A. B.; Moiseenkov, A. M.; Filippova, T. M.; Obol'nikova, E. A.; Samokhvalov, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 3 p. 594 - 599
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 3 p. 695 - 701
反应条件
1: 96 percent / 1.) n-BuLi / tetrahydrofuran; hexane / 0.5 h / -70 °C 2: 1.) Li, NH3, 2.) FeCl3, air / 1.) Et2O, -40 deg C, 3 h, 2.) AcOH, 25 deg C View Scheme
参考文献
Veselovskii, A. B.; Moiseenkov, A. M.; Filippova, T. M.; Obol'nikova, E. A.; Samokhvalov, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 3 p. 594 - 599
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 3 p. 695 - 701
