2-氯-N,N-二乙基苯甲酰胺合成路线 （共 8 条）
反应条件
N-chloro-succinimide; silica gel in acetonitrile T=150°C; 0.166667 h; microwave irradiation;
参考文献
Zhao, Zhongdong; Snieckus, Victor
Organic Letters, 2005 , vol. 7, # 13 p. 2523 - 2526
反应条件
1: oxalyl chloride / DMF / CH2Cl2 / 2.5 h 2: CH2Cl2 / 16 h View Scheme
参考文献
Kuliev; Kurbanov; Mamedov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 1 pt 2 p. 139 - 142
参考文献
Kuliev; Kurbanov; Mamedov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 1 pt 2 p. 139 - 142
反应条件
pyridine in dichloromethane Substitution; 20 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
参考文献
Geigy A.G.
Patent: US2551891 , 1949 ;
参考文献
Geigy A.G.
Patent: US2551891 , 1949 ;
反应条件
1: With disodium hydrogenphosphate in acetonitrile T=20°C; Methylation; 2: With sodium hydrogencarbonate Hydrolysis; 18 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
1: N,N-Diethyl-2-chlorobenzamide With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in tetrahydrofuran; cyclohexane
T=-78°C; 0.5 h;
2: dimethyl-disulfide in tetrahydrofuran; cyclohexane
T=-78 - 20°C;
参考文献
Mukherjee, Chandrani; Kamila, Sukanta; De, Asish
Tetrahedron, 2003 , vol. 59, # 26 p. 4767 - 4774
