烯丙基-四-O-乙酰基-beta-D-吡喃葡萄糖苷合成路线 (共 38 条)
反应条件
copper(II) sulfate; mercury dibromide; mercury(II) oxide in chloroform T=0 - 20°C; 10 h;
参考文献
Canadian Journal of Chemistry, , vol. 89, # 8 p. 959 - 963
反应条件
anhydrous iron chloride in dichloromethane T=20°C; 8 h; Inert atmosphereGreen chemistry; Reagent/catalystSolventTemperature; stereoselective reaction;
参考文献
Journal of the Brazilian Chemical Society, , vol. 23, # 11 p. 1982 - 1988
反应条件
zinc(II) chloride in toluene T=5 - 80°C; 2 h; Large scale; SolventReagent/catalystTemperatureTime;
参考文献
Organic Process Research and Development, , vol. 8, # 3 p. 405 - 407
反应条件
1: glucose pentaacetate With boron trifluoride diethyl etherate in dichloromethane T=20°C; 1 h; 2: allyl alcohol in dichloromethane T=20°C; 4 h;
参考文献
Chemistry and Physics of Lipids, , vol. 114, # 2 p. 139 - 147
反应条件
quinoline; hydrogen; Lindlar's catalyst in methanol 8 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 307, # 3-4 p. 351 - 354
反应条件
1: allyl alcohol; 1,2,3,4,6-penta-O-acetyl-β-D-glucopyranose With trimethylsilyl trifluoromethanesulfonate in dichloromethane T=0 - 20°C; 16 h; 2: With water; triethylamine in dichloromethane 3: acetic anhydride With pyridine T=20°C; 12 h; Inert atmosphere; optical yield given as percent de;
参考文献
Carbohydrate Research, , vol. 357, p. 147 - 150
反应条件
indium(III) chloride in dichloromethane T=30°C; 4.5 h;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 42, # 3 p. 602 - 604
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine T=20°C; 1 h;
参考文献
Tetrahedron, , vol. 61, # 44 p. 10559 - 10568
反应条件
1: 92 percent / BF3*OEt2 / CH2Cl2 / 2 h / Ambient temperature 2: 98 percent / H2, quinoline / 5percent Pd-CaCO3 / methanol / 8 h / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 307, # 3-4 p. 351 - 354
反应条件
silver(l) oxide in diethyl ether Inert atmosphere;
参考文献
Organic Process Research and Development, , vol. 4, # 1 p. 34 - 42