苯甲基 BETA-D-吡喃葡萄糖苷 2,3,4,6-四乙酸酯合成路线 （共 54 条）
反应条件
1: benzyl alcohol With silver carbonate in dichloromethane 2 h; Molecular sieveDarknessReflux; 2: 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide in dichloromethane 24 h; DarknessReflux;
参考文献
Cai, Ji-Bao; Hui, Li; Shen, Xia; Su, Qing-De
Asian Journal of Chemistry, 2010 , vol. 22, # 9 p. 6647 - 6651
反应条件
Amberlyst 15 in diethyl ether T=20°C; 3 h;
参考文献
Tian, Qiang; Zhang, Shuo; Yu, Qian; He, Mei-Bo; Yang, Jin-Song
Tetrahedron, 2007 , vol. 63, # 10 p. 2142 - 2147
反应条件
tin(IV) chloride in dichloromethane Substitution;
参考文献
Gomez, Ana M.; Danelon, Gerardo O.; Valverde, Serafin; Lopez, J. Cristobal
Carbohydrate Research, 1999 , vol. 320, # 1-2 p. 138 - 142
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-20°C; 0.833333 h;
参考文献
Li; Cai
Synthetic Communications, 1992 , vol. 22, # 14 p. 2121 - 2124
反应条件
1: 99 percent / HBr; AcOH / CH2Cl2 / 0 - 20 °C 2: 68 percent / Ag2CO3; I2 / CH2Cl2 / 15 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 33 p. 9756 - 9767
反应条件
mercury(II) cyanide in nitromethane
参考文献
Koto, Shinkiti; Morishima, Naohiko; Shichi, Sonoko; Haigoh, Hisamitsu; Hirooka, Motoko; et al.
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 12 p. 3257 - 3274
反应条件
silver carbonate in diethyl ether; dichloromethane T=20°C; 10 h; Molecular sieveInert atmosphereDarkness;
参考文献
Guo, Yibing; Zhao, Yahong; Zheng, Cheng; Meng, Ying; Yang, Yumin
Chemical and Pharmaceutical Bulletin, 2010 , vol. 58, # 12 p. 1627 - 1629
反应条件
silver(l) oxide in benzene
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 34, p. 2341 - 2353
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane Ambient temperature;
参考文献
Prata, Caria; Mora, Nathalie; Lacombe, Jean-Michel; Maurizis, Jean Claude; Pucci, Bernard
Tetrahedron Letters, 1997 , vol. 38, # 51 p. 8859 - 8862
参考文献
Straubinger, Markus; Knapp, Holger; Oka, Noriaki; Watanabe, Naoharu; Winterhalter, Peter
Journal of Agricultural and Food Chemistry, 1997 , vol. 45, # 10 p. 4053 - 4056
