2-氨基-6-甲氧基羰基苯甲酸合成路线 （共 5 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=2068.6 Torr; 8 h; Ambient temperature;
参考文献
Rogers, Miriam E.; Averill, Bruce A.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3308 - 3314
反应条件
hydrogenchloride T=20 - 60°C; 17 h;
参考文献
NOVARTIS AG; BAETTIG, Urs; BRUCE, Ian; PRESS, Neil John; WATSON, Simon James
Patent: WO2010/63802 A1, 2010 ;
Location in patent: Page/Page column 45 ;
WO 2010/063802 A1
反应条件
1: 77 percent / HCl / methanol / Heating 2: 92 percent / H2 / 5percent Pd/C / methanol / 8 h / 2068.6 Torr / Ambient temperature View Scheme
参考文献
Rogers, Miriam E.; Averill, Bruce A.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3308 - 3314
参考文献
Bogert; Jouard
Journal of the American Chemical Society, 1909 , vol. 31, p. 489
反应条件
1: 10 percent / isoamyl nitrite / 1,2-dimethoxy-ethane / Heating
2: 79 percent / ennecarbonyldiiron / benzene / Heating
View Scheme
参考文献
Giles, Robin G. F.; Sargent, Melvyn V.; Sianipar, Hercules
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 6 p. 1571 - 1579
