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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
10324-58-0
合成路线
(共 7 条)
10324-58-0
→
反应条件
1802-20-6
3-戊基吡啶
反应条件
chromium; silica gel; nickel; copper; sodium sulfate T=380 - 400°C;
参考文献
Tereshko, A. B.; Tarasevich, V. A.; Kozlov, N. G.
Russian Journal of Organic Chemistry, 1994 , vol. 30, # 9.2 p. 1512
Zhurnal Organicheskoi Khimii, 1994 , vol. 30, # 9 p. 1438
10324-58-0
→
反应条件
110-89-4
哌啶
+
21928-58-5
+
55275-24-6
+
110-58-7
正戊胺
+
2050-92-2
二戊胺
+
109-66-0
戊烷油
反应条件
hydrogen; sulphidized CoO-MoO3 T=300°C; P=37503 Torr; 1 h; prolonged (9 h) heating affords additional N-(1-butyl)piperidine, N-(1-ethyl)piperidine, and decane; MechanismProduct distribution;
参考文献
Cerny, Mirko
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 8 p. 2215 - 2218
10324-58-0
→
反应条件
110-89-4
哌啶
+
21928-58-5
+
55275-24-6
+
110-58-7
正戊胺
+
2050-92-2
二戊胺
+
109-66-0
戊烷油
反应条件
hydrogen; sulphidized CoO-MoO3 T=300°C; P=37503 Torr; 1 h; prolonged (9 h) heating affords additional N-(1-butyl)piperidine, N-(1-ethyl)piperidine, and decane; MechanismProduct distribution;
参考文献
Cerny, Mirko
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 8 p. 2215 - 2218
10324-58-0
→
反应条件
110-89-4
哌啶
+
21928-58-5
+
55275-24-6
+
110-58-7
正戊胺
+
2050-92-2
二戊胺
+
109-66-0
戊烷油
反应条件
hydrogen; sulphidized CoO-MoO3 T=300°C; P=37503 Torr; 1 h; prolonged (9 h) heating affords additional N-(1-butyl)piperidine, N-(1-ethyl)piperidine, and decane; MechanismProduct distribution;
参考文献
Cerny, Mirko
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 8 p. 2215 - 2218
10324-58-0
→
反应条件
110-89-4
哌啶
+
21928-58-5
+
55275-24-6
+
110-58-7
正戊胺
+
2050-92-2
二戊胺
+
109-66-0
戊烷油
反应条件
hydrogen; sulphidized CoO-MoO3 T=300°C; P=37503 Torr; 1 h; prolonged (9 h) heating affords additional N-(1-butyl)piperidine, N-(1-ethyl)piperidine, and decane; MechanismProduct distribution;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 45, # 8 p. 2215 - 2218
10324-58-0
→
反应条件
110-89-4
哌啶
+
21928-58-5
+
55275-24-6
+
110-58-7
正戊胺
+
2050-92-2
二戊胺
+
109-66-0
戊烷油
反应条件
hydrogen; sulphidized CoO-MoO3 T=300°C; P=37503 Torr; 1 h; prolonged (9 h) heating affords additional N-(1-butyl)piperidine, N-(1-ethyl)piperidine, and decane; MechanismProduct distribution;
参考文献
Cerny, Mirko
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 8 p. 2215 - 2218
10324-58-0
→
反应条件
110-89-4
哌啶
+
21928-58-5
+
55275-24-6
+
110-58-7
正戊胺
+
2050-92-2
二戊胺
+
109-66-0
戊烷油
反应条件
hydrogen; sulphidized CoO-MoO3 T=300°C; P=37503 Torr; 1 h; prolonged (9 h) heating affords additional N-(1-butyl)piperidine, N-(1-ethyl)piperidine, and decane; MechanismProduct distribution;
参考文献
Cerny, Mirko
Collection of Czechoslovak Chemical Communications, 1980 , vol. 45, # 8 p. 2215 - 2218