2-羟基-2-环己烯-1-酮合成路线 （共 68 条）
反应条件
trifluorormethanesulfonic acid in dichloromethane
Ambient temperature;
参考文献
Ponaras, A. A.; Meah, Md. Younus
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 4953 - 4956
反应条件
toluene-4-sulfonic acid in methanol
Heating;
参考文献
Harmata, Michael; Bohnert, Gary; Kuerti, Laszlo; Barnes, Charles L.
Tetrahedron Letters, 2002 , vol. 43, # 13 p. 2347 - 2349
反应条件
1: 23 percent / pTsOH / methanol / Heating
2: 71 percent / H(+) / benzene / Heating
View Scheme
参考文献
Harmata, Michael; Bohnert, Gary; Kuerti, Laszlo; Barnes, Charles L.
Tetrahedron Letters, 2002 , vol. 43, # 13 p. 2347 - 2349
参考文献
Utaka, Masanori; Hojo, Makoto; Fujii, Yasuyuki; Takeda, Akira
Chemistry Letters, 1984 , p. 635 - 638
反应条件
potassium carbonate in acetone
18 h; Heating;
参考文献
Feigenbaum, Alexandre; Pete, Jean-Pierre; Poquet-Dhimane, Anne
Tetrahedron Letters, 1988 , vol. 29, # 1 p. 73 - 74
反应条件
water; N-ethyl-N,N-diisopropylamine; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
0.166667 h; microwave irradiation, power 50 W;
参考文献
Garg, Neeraj; Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 4158 - 4162
反应条件
1: 42 percent / p-TsOH*H2O / benzene / 16 h / Heating
2: 86 percent / iPr2NEt, Ph3P, H2O / Pd(OAc)2 / dimethylformamide / 16 h / 100 °C
3: 84 percent / BBr3 / CH2Cl2 / 1.) -78 deg C, 1 h, 2.) -12 deg C, 3 h
View Scheme
参考文献
Garg, Neeraj; Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 4158 - 4162
反应条件
water; N-ethyl-N,N-diisopropylamine; triphenylphosphine; palladium diacetate in N,N-dimethyl-formamide
T=100°C; 16 h;
参考文献
Garg, Neeraj; Larhed, Mats; Hallberg, Anders
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 4158 - 4162
反应条件
oxygen; rose bengal in methanol
T=40°C; 13 h; Irradiation;
参考文献
Utaka, Masanori; Nakatani, Manabu; Takeda, Akira
Tetrahedron Letters, 1983 , vol. 24, # 8 p. 803 - 806
反应条件
oxygen; rose bengal
T=40°C; 13 h; Irradiation;
参考文献
Utaka, Masanori; Nakatani, Manabu; Takeda, Akira
Tetrahedron Letters, 1983 , vol. 24, # 8 p. 803 - 806
