(3,4-二甲氧基苯基)乙酰氯合成路线 （共 69 条）
反应条件
1: AlCl3; carbon disulfide
3: sodium-amalgam; ethanol; acetic acid
View Scheme
参考文献
Allen; Buck
Journal of the American Chemical Society, 1930 , vol. 52, p. 310,312
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 3 h / Reflux
2: selenium(IV) oxide / 1,4-dioxane; water / 15 h / Reflux
View Scheme
参考文献
Short, Rhys; Carta, Mariolino; Bezzu, C. Grazia; Fritsch, Detlev; Kariuki, Benson M.; McKeown, Neil B.
Chemical Communications, 2011 , vol. 47, # 24 p. 6822 - 6824
反应条件
tin(IV) chloride in dichloromethane
2 h; Ambient temperature;
参考文献
Arriortua, M. I.; Via, J.; Urtiaga, M. K.; Dominguez, E.; Igartua, A.; Sotomayor, N.
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 5 p. 361 - 366
反应条件
1: AlCl3 / nitrobenzene
2: HNO3 / acetic acid
3: K2CO3 / acetone
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参考文献
Faber; Wiegrebe
Helvetica chimica acta, 1976 , vol. 59, # 6 p. 2201 - 2212
反应条件
1: AlCl3; carbon disulfide
View Scheme
参考文献
Allen; Buck
Journal of the American Chemical Society, 1930 , vol. 52, p. 310,312
反应条件
1: 1 h
2: HNO3 / acetic acid / 1 h / 0 °C
View Scheme
参考文献
Swenton,J.S.; Bonke,B.R.; Chen,C-P.
Journal of Organic Chemistry, 1989 , vol. 54, p. 51
反应条件
sodium hydroxide in water
T=0°C; 1 h;
参考文献
Nagubandi, Sreeramulu; Fodor, G.
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 1457 - 1463
反应条件
1: AlCl3 / nitrobenzene
2: HNO3 / acetic acid
View Scheme
参考文献
Faber; Wiegrebe
Helvetica chimica acta, 1976 , vol. 59, # 6 p. 2201 - 2212
反应条件
1: dimethylformamide; potassium carbonate / Erwaermen des Reaktionsprodukts mit Lithiumalanat in Tetrahydrofuran
View Scheme
参考文献
Gruessner et al.
Helvetica Chimica Acta, 1957 , vol. 40, p. 1232,1238
