(3,4-二甲氧基苯基)乙酰氯合成路线 (共 69 条)
反应条件
thionyl chloride in dichloromethane
参考文献
Jetter, Michele C.; Youngman, Mark A.; McNally, James J.; McDonnell, Mark E.; Zhang, Sui-Po; Dubin, Adrienne E.; Nasser, Nadia; Codd, Ellen E.; Flores, Christopher M.; Dax, Scott L.
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 22 p. 6160 - 6163
反应条件
sodium hydroxide; thionyl chloride in methanol; dichloromethane; chloroform
反应条件
triethylamine in chloroform
反应条件
thionyl chloride in benzene
参考文献
US4529604 A1, ;
US 4529604 A
反应条件
in 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran; N,N-dimethyl-formamide
反应条件
1: aq. Ag2O / dioxane 2: (COCl)2; DMF / CH2Cl2 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 15 p. 1723 - 1727
反应条件
1: (COCl)2; DMF / CH2Cl2 2: diethyl ether / 0 °C 3: aq. Ag2O / dioxane 4: (COCl)2; DMF / CH2Cl2 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 15 p. 1723 - 1727
反应条件
1: diethyl ether / 0 °C 2: aq. Ag2O / dioxane 3: (COCl)2; DMF / CH2Cl2 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 10, # 15 p. 1723 - 1727
反应条件
1: 74.2 percent / KOH / methanol; H2O / 5 h / Heating 2: oxalyl chloride / benzene / 1 h / Ambient temperature View Scheme
参考文献
Journal of the Indian Chemical Society, , vol. 66, # 8-10 p. 656 - 659