反应条件
CaH2 in cyclohexane react. under N2, suspending the trialkoxyborane , B(OH)3 and CaH2 in cyclohexane, stirring for 1 h at room temp., heating to 80-90°C overnight; hot filtration under N2, washing with hot cyclohexane, evapn.;
参考文献
Cole, T. E.; Quintanilla, R.; Rodewald, S.
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1990 , vol. 20, p. 55 - 64