aluminium trichloride; aluminium
35°C; ratio of obtained isomers 4.6 : 1 = para : meta;
参考文献
Muetterties,E.L.
Journal of the American Chemical Society, 1960 , vol. 82, p. 4163 - 4166
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Gmelin Handbook: B: B-Verb.9, 5.2.6, page 205 - 215
Soulie, J.; Cadiot, P.
Bulletin de la Societe Chimique de France, 1966 , p. 1981 - 1992
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Gmelin Handbook: B: B-Verb.13, 4.7.2.5, page 209 - 219
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Gmelin Handbook: B: B-Verb.9, 5.2.6, page 205 - 215
byproducts: boron hydride; High Pressure; under N2; diborane and trihalogen-borane was added to toluene at -130°C, then in a closed autoclave the mixture was heated to 120°C for 90 min; at -195.8°C H2 was removed, at room temp. the residue of trihalogen-borane and diborane were removed;
Muetterties,E.L.
Journal of the American Chemical Society, 1960 , vol. 82, p. 4163 - 4166
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Muetterties
Journal of the American Chemical Society, 1959 , vol. 81, p. 2597
Gerrard, W.; Howarth, M.; Mooney, E. F.; Pratt, D. E.
Journal of the Chemical Society, 1963 , p. 1582 - 1584
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Gmelin Handbook: B: B-Verb.9, 5.2.6, page 205 - 215
byproducts: boron hydride; High Pressure; under N2; diborane and trihalogen-borane was added to p-xylene at -130°C, then in a closed autoclave the mixture was heated to 130°C; at -195.8°C H2 was removed, at room temp. the residue of trihalogen-borane and diborane were removed;