2-溴-N-苯基苯甲酰胺合成路线 （共 21 条）
反应条件
2,2'-azo-bisisobutyronitrile; potassium tert-butylate in benzene T=110°C; 6 h;
参考文献
Bhakuni, Bhagat Singh; Kumar, Amit; Balkrishna, Shah Jaimin; Sheikh, Javeed Ahmed; Konar, Sanjit; Kumar, Sangit
Organic Letters, 2012 , vol. 14, # 11 p. 2838 - 2841
反应条件
selenium; copper(l) iodide; 1,10-phenanthroline; potassium carbonate in N,N-dimethyl-formamide T=110°C; 16 h; Inert atmosphere;
参考文献
Balkrishna, Shah Jaimin; Bhakuni, Bhagat Singh; Chopra, Deepak; Kumar, Sangit
Organic Letters, 2010 , vol. 12, # 23 p. 5394 - 5397
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide T=100°C; 0.166667 h; Inert atmosphere;
参考文献
Kavala, Veerababurao; Wang, Cheng-Chuan; Barange, Deepak Kumar; Kuo, Chun-Wei; Lei, Po-Min; Yao, Ching-Fa
Journal of Organic Chemistry, 2012 , vol. 77, # 11 p. 5022 - 5029
反应条件
copper(l) iodide; caesium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine in N,N-dimethyl-formamide T=80°C; 24 h; Inert atmosphere;
参考文献
Xu, Lanting; Jiang, Yongwen; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 4 p. 1150 - 1153
反应条件
copper(l) iodide; caesium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine in N,N-dimethyl-formamide
T=80°C; 24 h; Inert atmosphere;
参考文献
Xu, Lanting; Jiang, Yongwen; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 4 p. 1150 - 1153
反应条件
1: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / N,N-dimethyl-formamide / 3 h / 120 °C / |Microwave irradiation; |Inert atmosphere
2: ammonium acetate; NaAuCl4*2H2O; silver hexafluoroantimonate / acetonitrile / 20 h / 85 °C
View Scheme
参考文献
Long, Yuhua; She, Zhigang; Liu, Xiaochen; Chen, Yu
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2579 - 2588
反应条件
1: copper(l) iodide; caesium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine / N,N-dimethyl-formamide / 24 h / 80 °C / Inert atmosphere
2: 1,1,1,3,3,3-hexamethyl-disilazane; zinc(II) chloride / N,N-dimethyl-formamide / 4 h / 20 °C
View Scheme
参考文献
Xu, Lanting; Jiang, Yongwen; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 4 p. 1150 - 1153
反应条件
[2-(8-methoxynaphthalen-1-yl)phenyl]diphenylphosphane; caesium carbonate; palladium diacetate in 1,4-dioxane
T=100°C; 24 h;
参考文献
Furuta, Takumi; Kitamura, Yuki; Hashimoto, Ayano; Fujii, Satoshi; Tanaka, Kiyoshi; Kan, Toshiyuki
Organic Letters, 2007 , vol. 9, # 2 p. 183 - 186
反应条件
palladium diacetate; sodium carbonate; cesium fluoride; bis(1,1-diphenylphosphino)methane in toluene; acetonitrile
T=20 - 110°C;
参考文献
Lu, Chun; Dubrovskiy, Anton V.; Larock, Richard C.
Journal of Organic Chemistry, 2012 , vol. 77, # 19 p. 8648 - 8656
反应条件
copper(l) iodide; caesium carbonate in dimethyl sulfoxide
T=100°C; 0.166667 h; Inert atmosphere;
参考文献
Kavala, Veerababurao; Wang, Cheng-Chuan; Barange, Deepak Kumar; Kuo, Chun-Wei; Lei, Po-Min; Yao, Ching-Fa
Journal of Organic Chemistry, 2012 , vol. 77, # 11 p. 5022 - 5029
