(9H-芴-9-基)甲基 2,5-二氧代吡咯烷-1-羧酸合成路线 (共 36 条)
反应条件
triethylamine in water; acetonitrile 1 h;
参考文献
Echner, Hartmut; Voelter, Wolfgang
Liebigs Annalen der Chemie, 1988 , p. 1095 - 1098
反应条件
triethylamine in water; acetonitrile 1 h;
参考文献
Echner, Hartmut; Voelter, Wolfgang
Liebigs Annalen der Chemie, 1988 , p. 1095 - 1098
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water T=20°C;
参考文献
Byrne, Cillian; McEwan, Paul A.; Emsley, Jonas; Fischer, Peter M.; Chan, Weng C.
Chemical Communications, 2011 , vol. 47, # 9 p. 2589 - 2591
反应条件
in ethylene glycol dimethyl ether; water 18 h; Ambient temperaturepH 9.0-9.5; Yield given;
参考文献
Wysong, Christopher L.; Yokum, T. Scott; Morales, Guillermo A.; Gundry, Rebekah L.; McLaughlin, Mark L.; Hammer, Robert P.
Journal of Organic Chemistry, 1996 , vol. 61, # 22 p. 7650 - 7651
反应条件
potassium carbonate in 1,4-dioxane T=20°C;
参考文献
MAX-PLANCK-GESELLSCHAFT ZUR FÖRDERUNG DER WISSENSCHAFTEN E.V.; GOPALAKRISHNAN, Ranganath; HAUSCH, Felix
Patent: WO2013/91900 A1, 2013 ;
Location in patent: Page/Page column 41 ;
反应条件
sodium carbonate; toluene-4-sulfonic acid 1) dioxane, gas pressure: 350 mbar, 3 d, r.t., 2) dioxane, 0 deg C to r.t., 14 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lajoie; Crivici; Adamson
Synthesis, 1990 , # 7 p. 571 - 572
反应条件
triethylamine in water; acetonitrile
参考文献
Elsaesser, Celine; Monien, Bernhard; Haehnel, Wolfgang; Bittl, Robert
Magnetic Resonance in Chemistry, 2005 , vol. 43, # SPEC. ISS. p. S26-S33
反应条件
sodium hydrogencarbonate in water; acetone Acylation; 3 h;
参考文献
Wojczewski, Christian; Schwarzer, Karin; Engels, Joachim W.
Helvetica Chimica Acta, 2000 , vol. 83, # 6 p. 1268 - 1277
反应条件
triethylamine in water; acetonitrile 1 h;
参考文献
Echner, Hartmut; Voelter, Wolfgang
Liebigs Annalen der Chemie, 1988 , p. 1095 - 1098
反应条件
sodium carbonate; toluene-4-sulfonic acid 1) dioxane, gas pressure: 350 mbar, 3 d, r.t., 2) dioxane, 0 deg C to r.t., 14 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lajoie; Crivici; Adamson
Synthesis, 1990 , # 7 p. 571 - 572