[(3-甲基丁-2-烯-1-基)硫代]苯合成路线 （共 66 条）
反应条件
1: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O 2: Na, ethanol / Ambient temperature 3: 40 percent / hydrogen / RuO2*nH2O / methanol / 48 h / 60 °C / 6080 Torr View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
反应条件
1: 75.8 percent / 85percent H3PO4, P2O5 / benzene / 20 h / Heating 2: 60.3 percent / SnCl4 / benzene / 5 h / Ambient temperature View Scheme
参考文献
Dawson, Marcia I.; Hobbs, Peter D.; Derdzinski, Krzysztof; Chan, Rebecca L.-S.; Gruber, John; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 11 p. 1516 - 1531
反应条件
1: 81 percent / 1.) n-BuLi, HMPA / tetrahydrofuran; hexane / 2.) -70 deg C, 15 min 2: 1.) Li, NH3, 2.) air, FeCl3 / 1.) ether, -70 deg C, 15 min, 2.) AcOH View Scheme
参考文献
Veselovskii, A. B.; Moiseenkov, A. M.; Filippova, T. M.; Obol'nikova, E. A.; Samokhvalov, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 3 p. 594 - 599
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 3 p. 695 - 701
反应条件
1: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O 2: Na, ethanol / Ambient temperature View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
反应条件
anhydrous lithium acetate; copper diacetate; copper T=85 - 90°C;
参考文献
Tetrahedron Letters, , vol. 25, # 5 p. 541 - 542
反应条件
hydrogen; lt;Ru3O(CH3COO)6(H2O)3gt;(1+)*CH3COO(1-) in N,N-dimethyl-formamide T=80°C; P=3040 Torr; 2 h; other catalyst: RuO2*nH2O;
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
反应条件
1: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O 2: Na, ethanol / Ambient temperature 3: hydrogen / <Ru3O(CH3COO)6(H2O)3>(1+)*CH3COO(1-) / dimethylformamide / 2 h / 80 °C / 3040 Torr / other catalyst: RuO2*nH2O View Scheme
参考文献
Cere, Vanda; Massaccesi, Franco; Pollicino, Salvatore; Ricci, Alfredo
Synthetic Communications, 1996 , vol. 26, # 5 p. 899 - 907
反应条件
sodium hydride in ethylene glycol dimethyl ether
a) 0 deg C, 1 h, b) RT, 16 h;
参考文献
Pace, Vittorio; Castoldi, Laura; Holzer, Wolfgang
Tetrahedron Letters, 2012 , vol. 53, # 8 p. 967 - 972
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; carbon monoxide in dichloromethane
T=110°C; Addition; P=20686.5 Torr; 60 h;
参考文献
Xiao; Vasapollo; Alper
Journal of Organic Chemistry, 2000 , vol. 65, # 13 p. 4138 - 4144
反应条件
1: thiophenol With sodium hydride in N,N-dimethyl-formamide
T=20°C; 0.166667 h;
2: 3-methyl-but-2-en-1-yl acetate With tetrakis(triethylphosphite)nickel(O) in tetrahydrofuran; N,N-dimethyl-formamide
20 h; Heating; Further stages.;
参考文献
Yatsumonji, Yasutaka; Ishida, Yusuke; Tsubouchi, Akira; Takeda, Takeshi
Organic Letters, 2007 , vol. 9, # 22 p. 4603 - 4606
