2-(乙基硫代)-1-苯基乙酮合成路线 （共 20 条）
反应条件
1.1: copper(I) bromide / ethanol / 60 °C / |Inert atmosphere 2.1: sodium methylate / methanol / 0.08 h / |Inert atmosphere 2.2: |Inert atmosphere View Scheme
参考文献
Su, Qiong; Zhao, Zi-Jian; Xu, Feng; Lou, Peng-Cai; Zhang, Kai; Xie, De-Xun; Shi, Lei; Cai, Qing-Yun; Peng, Zhi-Hong; An, De-Lie
European Journal of Organic Chemistry, 2013 , # 8 p. 1551 - 1557
参考文献
Sulko, Jerzy
Acta Poloniae Pharmaceutica - Drug Research, 1997 , vol. 54, # 4 p. 319 - 324
反应条件
sodium methylate in methanol 1 h; Ambient temperature;
参考文献
Boeykens, Marc; De Kimpe, Norbert
Tetrahedron, 1994 , vol. 50, # 43 p. 12349 - 12360
反应条件
Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Vedejs, E.; Stults, J. S.; Wilde, R. G.
Journal of the American Chemical Society, 1988 , vol. 110, # 16 p. 5452 - 5460
参考文献
Nagao,Y. et al.
Tetrahedron Letters, 1977 , p. 1345 - 1348
反应条件
1.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 0.5 h / -78 °C / |Inert atmosphere 1.2: 0.5 h / -78 - 20 °C / |Inert atmosphere 2.1: lithium hexamethyldisilazane / tetrahydrofuran; ethylbenzene / 1 h / -78 °C / |Inert atmosphere View Scheme
参考文献
Su, Qiong; Zhao, Zi-Jian; Xu, Feng; Lou, Peng-Cai; Zhang, Kai; Xie, De-Xun; Shi, Lei; Cai, Qing-Yun; Peng, Zhi-Hong; An, De-Lie
European Journal of Organic Chemistry, 2013 , # 8 p. 1551 - 1557
反应条件
Ambient temperatureIrradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Vedejs, E.; Stults, J. S.; Wilde, R. G.
Journal of the American Chemical Society, 1988 , vol. 110, # 16 p. 5452 - 5460
反应条件
thallium(III) nitrate
参考文献
Nagao,Y. et al.
Tetrahedron Letters, 1977 , p. 1345 - 1348
反应条件
selenium(IV) oxide; dihydrogen peroxide in methanol
T=15°C; 3 h;
参考文献
Olivato, Paulo Roberto; Bonfada, Elida; Rittner, Roberto
Magnetic Resonance in Chemistry, 1992 , vol. 30, # 1 p. 81 - 84
反应条件
sodium periodate in acetonitrile
Ambient temperature;
参考文献
Olivato, Paulo Roberto; Bonfada, Elida; Rittner, Roberto
Magnetic Resonance in Chemistry, 1992 , vol. 30, # 1 p. 81 - 84
