7-甲氧基-2,2-二苯基-1,3-苯并二氧代-5-羧酸甲酯合成路线 (共 9 条)
反应条件
potassium carbonate in diethyl ether; acetone T=20°C; Methylation;
参考文献
Hodgson, Jonathan M.; Morton, Lincoln W.; Puddey, Ian B.; Beilin, Lawrence J.; Croft, Kevin D.
Journal of Agricultural and Food Chemistry, 2000 , vol. 48, # 6 p. 2276 - 2280
反应条件
1: 70 percent / K2CO3 / 0.17 h / 170 - 180 °C 2: 92 percent / K2CO3 / diethyl ether; acetone / 20 °C View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 48, # 6 p. 2276 - 2280
反应条件
1: 33.6 g / 0.08 h / 170 - 180 °C 2: 30.8 g / K2CO3 / acetone / 10 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 10 p. 2733 - 2736
反应条件
methanol; sodium ethanolate
参考文献
Journal of the Chemical Society, , p. 796,811
参考文献
Benard, Christophe; Zouhiri, Fatima; Normand-Bayle, Marie; Danet, Michele; Desmaele, Didier; Leh, Herve; Mouscadet, Jean-Francois; Mbemba, Gladys; Thomas, Claire-Marie; Bonnenfant, Sabine; Le Bret, Marc; D'Angelo, Jean
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 10 p. 2473 - 2476
反应条件
1: HCl 2: 70 percent / K2CO3 / 0.17 h / 170 - 180 °C 3: 92 percent / K2CO3 / diethyl ether; acetone / 20 °C View Scheme
参考文献
Journal of Agricultural and Food Chemistry, , vol. 48, # 6 p. 2276 - 2280
参考文献
Hodgson, Jonathan M.; Morton, Lincoln W.; Puddey, Ian B.; Beilin, Lawrence J.; Croft, Kevin D.
Journal of Agricultural and Food Chemistry, 2000 , vol. 48, # 6 p. 2276 - 2280
参考文献
Hodgson, Jonathan M.; Morton, Lincoln W.; Puddey, Ian B.; Beilin, Lawrence J.; Croft, Kevin D.
Journal of Agricultural and Food Chemistry, 2000 , vol. 48, # 6 p. 2276 - 2280
反应条件
1: aqueous hydrochloric acid
2: zinc chloride / anschliessend Behandeln mit wss. Kaliumhydrogencarbonat
3: chloroform; phosphorus (V)-chloride
View Scheme
参考文献
Bradley; Robinson; Schwarzenbach
Journal of the Chemical Society, 1930 , p. 796,811