3-甲基-2-苯基-1H-吲哚合成路线 （共 60 条）
反应条件
potassium carbonate; triphenylphosphine; lithium chloride; palladium diacetate in N,N-dimethyl-formamide
参考文献
Boehringer Ingelheim (Canada) Ltd.
Patent: US2003/176433 A1, 2003 ;
反应条件
potassium carbonate; palladium diacetate in N,N-dimethyl-formamide
T=130°C; 30 h;
参考文献
Cui, Xin; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 21 p. 3458 - 3462
反应条件
potassium carbonate; palladium diacetate in N,N-dimethyl-formamide
T=130°C; 30 h;
参考文献
Cui, Xin; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 21 p. 3458 - 3462
反应条件
iron(II) chloride in tetrahydrofuran
T=70°C; 24 h; Inert atmosphere;
参考文献
Jana, Samaresh; Clements, MacK D.; Sharp, Barry K.; Zheng, Nan
Organic Letters, 2010 , vol. 12, # 17 p. 3736 - 3739
反应条件
C29H31Cl2FeN3Pd; tetrabutylammomium bromide; potassium carbonate in 1,4-dioxane
T=140°C; Larock Annulation; 24 h; regioselective reaction;
参考文献
He, Pan; Du, Yufeng; Liu, Gang; Cao, Changsheng; Shi, Yanhui; Zhang, Juan; Pang, Guangsheng
RSC Advances, 2013 , vol. 3, # 40 p. 18345 - 18350
反应条件
C70H44Cl2F64N2O6Pd2; tetrabutylammomium bromide; sodium carbonate in water
T=150°C; 0.466667 h; Microwave irradiationGreen chemistry; regioselective reaction;
参考文献
Ang, Wei Jie; Tai, Chih-Hsuan; Lo, Lee-Chiang; Lam, Yulin
RSC Advances, 2014 , vol. 4, # 10 p. 4921 - 4929
反应条件
1: With Cp*Rh(H2O)3(OTf)2; oxygen; acetic anhydride in 1,1-dimethylpropan-1-ol
T=100°C; P=760.051 Torr; 24 h; Inert atmosphereSchlenk technique;
2: With sodium hydroxide in methanol; 1,1-dimethylpropan-1-ol
T=20°C; 1 h;
参考文献
Zhang, Guoying; Yu, Hui; Qin, Guiping; Huang, Hanmin
Chemical Communications, 2014 , vol. 50, # 33 p. 4331 - 4334
反应条件
sulfuric acid in tetrahydrofuran
Fischer indolization; Wagner-Meerwein rearran.; 3 h; Heating;
参考文献
Angelovski, Goran; Keraenen, Mark D.; Linnepe, Petra; Grudzielanek, Stefan; Eilbracht, Peter
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1193 - 1199
反应条件
[(η5-C5Me5)2Rh2(μ-Cl)2Cl2]; sodium acetate; acetic acid; pentan-3-one in ethanol
T=110°C; 20 h; Sealed tubeInert atmosphere; regioselective reaction;
参考文献
Muralirajan, Krishnamoorthy; Cheng, Chien-Hong
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 7 p. 1571 - 1576
反应条件
copper(l) chloride
T=270°C;
参考文献
Verkade; Janetzky
Recueil des Travaux Chimiques des Pays-Bas, 1943 , vol. 62, p. 775,780
Full Text Show Details
Arbusow; Saizew; Rasumow
Chemische Berichte, 1935 , vol. 68, p. 1792
Zhurnal Obshchei Khimii, 1936 , vol. 6, p. 289
