二甲基3,4,5,6-四氟邻苯二甲酸酯合成路线 (共 6 条)
反应条件
hydrogenchloride; potassium fluoride; triethylamine in methanol; n-heptane; water; toluene
参考文献
Warner-Lambert Company
Patent: US4885386 A1, 1989 ;
反应条件
in methanol; sulfuric acid
参考文献
Daiichi Pharmaceutical Co., Ltd.
Patent: US5849757 A1, 1998 ;
反应条件
in dichloromethane; toluene
参考文献
Lemal, David M.; Ramanathan, Sudharsanam; Shellito, John
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3392 - 3396
参考文献
Medina, Carlos Perez; Lopez, Concepcion; Claramunt, Rosa M.; Elguero, Jose
European Journal of Organic Chemistry, 2010 , # 5 p. 890 - 899
反应条件
(i) nBuLi, (ii) /BRN= 635821/, (iii) aq. H2SO4; Multistep reaction;
参考文献
Chambers,R.D.; Spring,D.J.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 2394 - 2397
反应条件
hydrogenchloride; sulfuric acid in water; acetic acid
参考文献
Warner-Lambert Company
Patent: US4782180 A1, 1988 ;