1: (i) NaH, THF, (ii) Al-Hg, aq. THF 2: (i) NaH, DMF, (ii) /BRN= 1722657/ 3: H2 / Pd-CaCO3 / ethanol / 76000 Torr / Ambient temperature 4: (i) NaH, THF, (ii) Al-Hg, aq. THF View Scheme

1: (i) NaH, THF, (ii) Al-Hg, aq. THF 2: (i) NaH, DMF, (ii) /BRN= 1722657/ 3: H2 / Pd-CaCO3 / ethanol / 76000 Torr / Ambient temperature 4: (i) NaH, THF, (ii) Al-Hg, aq. THF 5: (i) NaH, THF, (ii) /BRN= 1724987/ 6: LiAlH4 / diethyl ether View Scheme

(i) NaH, THF, (ii) Al-Hg, aq. THF; Multistep reaction;

1: (i) NaH, THF, (ii) Al-Hg, aq. THF 2: (i) NaH, DMF, (ii) /BRN= 1722657/ 3: H2 / Pd-CaCO3 / ethanol / 76000 Torr / Ambient temperature 4: (i) NaH, THF, (ii) Al-Hg, aq. THF View Scheme

Multi-step reaction with 3 steps 1: (i) NaH, THF, (ii) Al-Hg, aq. THF2: (i) NaH, DMF, (ii) /BRN= 1722657/3: H2 / Pd-CaCO3 / ethanol / 76000 Torr / Ambient temperature