O,O-双(2-羟基乙氧基)苯合成路线 （共 18 条）
反应条件
2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane in ethanol 2 h; Heatinginfluence of different crown ethers, catalytic activity of crown ethers; Product distribution;
参考文献
Draye, Micheline; Favre-Reguillon, Alain; Chomel, Rodolph; Faure, Rene; Guy, Alain; Foos, Jacques; Lemaire, Marc
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 2 p. 183 - 197
反应条件
anhydrous diethylamine hydrochloride T=30 - 35°C; 240 h;
参考文献
Topal; Demirel; Togrul; Turgut; Hosgoeren
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 1 p. 281 - 284
反应条件
anion exchange resin A (Cl-type) in toluene T=100°C; 1.5 - 3.5 h;
参考文献
US2004/181099 A1, ;
Page 15-16 ;
反应条件
diaionreg; TSA1200 in 2-methoxy-ethanol T=100°C; 9 h;
参考文献
US2004/181099 A1, ;
Page 17-19 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 0.5 h; Heating;
参考文献
Brown; Foubister
Journal of Medicinal Chemistry, 1983 , vol. 26, # 4 p. 590 - 592
反应条件
hydrogenchloride in methanol; dichloromethane 1 h; Ambient temperature;
参考文献
Czech, Bronislaw P.; Czech, Anna; Knudsen, Brian E.; Bartsch, Richard A.
Gazzetta Chimica Italiana, 1987 , vol. 117, # 12 p. 717 - 722
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Reduction; 1.5 h; Heating;
参考文献
Hijfte, Luc Van; Zerr, Veronique; Hibert, Marcel; Giersbergen, Paul L.M. van
Med. Chem. Res., 1995 , vol. 5, # 6 p. 449 - 454
反应条件
1: 1) aq. NaOH / 1) EtOH, 30 min, 2) EtOH, heating 2: 87 percent / H2 / 10percent Pd/C / ethyl acetate / 4 h / 2280 Torr / Ambient temperature View Scheme
参考文献
Chemische Berichte, , vol. 118, # 11 p. 4439 - 4452
反应条件
potassium carbonate in acetone 24 h; Heating;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 2 p. 183 - 197
反应条件
1: 50 percent / 65percent nitric acid / CHCl3 / 0.5 h / 20 - 24 °C 2: 75 percent / 60percent aq. KOH / dicyclohexyl-18-crown-6 / tetrahydrofuran / 5 h / Heating View Scheme
参考文献
Abakumova, N. I.; Kolenko, I. K.; Kodess, M. I.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1305 - 1307
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 7 p. 1495 - 1498
