2-溴-6-甲基-4-硝基苯胺合成路线 (共 6 条)
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide; calcium carbonate in methanol; dichloromethane 0.5 h; Ambient temperature;
参考文献
Kajigaeshi, Shoji; Kakinami, Takaaki; Inoue, Kazuhisa; Kondo, Manabu; Nakamura, Hiroko; et al.
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 2 p. 597 - 599
反应条件
bromine 1 h; Ambient temperature;
参考文献
O'Neill, Paul M.; Willock, David J.; Hawley, Shaun R.; Bray, Patrick G.; Storr, Richard C.; Ward, Stephen A.; Park, B. Kevin
Journal of Medicinal Chemistry, 1997 , vol. 40, # 4 p. 437 - 448
参考文献
Bulletin de la Societe Chimique de France, , vol. <4>35, p. 1328
参考文献
Nevile; Winther
Chemische Berichte, 1880 , vol. 13, p. 963
Chemische Berichte, 1881 , vol. 14, p. 417
反应条件
1: Diazotization.Erwaermen des Diazoniumperbromids mit Eisessig
2: iron; acetic acid
3: alcohol; nitrous acid
4: diluted nitric acid / 130 °C
View Scheme
参考文献
Nevile; Winther
Chemische Berichte, 1880 , vol. 13, p. 963
Chemische Berichte, 1881 , vol. 14, p. 417
反应条件
1: Diazotization.Erwaermen des Diazoniumperbromids mit Eisessig
2: iron; acetic acid
3: alcohol; nitrous acid
View Scheme
参考文献
Nevile; Winther
Chemische Berichte, 1880 , vol. 13, p. 963
Chemische Berichte, 1881 , vol. 14, p. 417