6-甲基-2-苯基苯并噻唑合成路线 （共 39 条）
反应条件
potassium permanganate; sulfuric acid; acetic acid
参考文献
Fridman
Zhurnal Obshchei Khimii, 1950 , vol. 20, p. 1807,1811; engl. Ausg. S. 1871, 1874, 1875
反应条件
in der Kalischmelze;
参考文献
Pfitzinger; Gattermann
Chemische Berichte, 1889 , vol. 22, p. 1066
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in 2,2,2-trifluoroethanol
T=20°C; 0.5 h;
参考文献
Downer-Riley, Nadale K.; Jackson, Yvette A.
Tetrahedron, 2008 , vol. 64, # 33 p. 7741 - 7744
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide
T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide
T=100°C; 12 h;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
oxygen in dimethyl sulfoxide; chlorobenzene
T=140°C; P=760.051 Torr; 16 h; Sealed tube;
参考文献
Liao, Yunfeng; Qi, Hongrui; Chen, Shanping; Jiang, Pengcheng; Zhou, Wang; Deng, Guo-Jun
Organic Letters, 2012 , vol. 14, # 23 p. 6004 - 6007
反应条件
1: With copper diacetate; potassium ethylxanthate in N,N-dimethyl-formamide
T=80°C; Ullmann type reaction; 15 h; Inert atmosphere;
2: With hydrogenchloride in water; N,N-dimethyl-formamide
T=20°C; 8 h; Inert atmosphere;
参考文献
Prasad; Sekar
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 10 p. 1659 - 1665
反应条件
tert.-butylhydroperoxide; potassium iodide in water
T=100°C; 8 h; Inert atmosphere;
参考文献
Gao, Yuyu; Song, Qiuling; Cheng, Guolin; Cui, Xiuling
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 7 p. 1044 - 1047
反应条件
dipotassium peroxodisulfate; FeCl3·6H2O in water; dimethyl sulfoxide
T=100°C; 12 h; Overall yield = 75 percent;
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
(R)-(+)-1,1'-binaphthyl-2,2'-diamine; caesium carbonate; copper dichloride in acetonitrile
T=110°C; 29 h; Inert atmosphere;
参考文献
Jaseer; Prasad; Dandapat, Arpan; Sekar, Govindasamy
Tetrahedron Letters, 2010 , vol. 51, # 38 p. 5009 - 5012
