(4-苯并噻唑-2-基-苯基)-二甲基-胺合成路线 （共 20 条）
参考文献
UNIVERSITY OF PITTSBURGH
Patent: US2003/236391 A1, 2003 ;
Location in patent: Page 16 ;
反应条件
Fe(HSO4)3 in ethanol
0.333333 h; Reflux; chemoselective reaction;
参考文献
Eshghi, Hossein; Rahimizadeh, Mohammad; Shiri, Ali; Sedaghat, Parisa
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 2 p. 515 - 518
反应条件
sodium hydroxide; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; [(t-Bu)3PH]BF4 in dimethyl sulfoxide
T=60°C; 24 h;
参考文献
Miyaoku, Takayuki; Mori, Atsunori
Heterocycles, 2009 , vol. 77, # 1 p. 151 - 155
反应条件
potassium carbonate in dimethyl sulfoxide
T=100°C; 16 h;
参考文献
UNIVERSITY OF PITTSBURGH
Patent: US2003/236391 A1, 2003 ;
Location in patent: Page 16 ;
反应条件
copper diacetate; triethylamine in ethanol
T=70°C; 6 h;
参考文献
Sun, Yadong; Jiang, Huanfeng; Wu, Wanqing; Zeng, Wei; Wu, Xia
Organic Letters, 2013 , vol. 15, # 7 p. 1598 - 1601
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in water
T=80°C; 0.666667 h;
参考文献
Boeini, Hassan Zali; Najafabadi, Khadijeh Hajibabaei
European Journal of Organic Chemistry, 2009 , # 29 p. 4926 - 4929
反应条件
magnesium sulfate; copper(l) chloride in dimethyl sulfoxide
T=110°C; 6 h;
参考文献
Park, Namjin; Heo, Yumi; Kumar, Manian Rajesh; Kim, Yong; Song, Kwang Ho; Lee, Sunwoo
European Journal of Organic Chemistry, 2012 , # 10 p. 1984 - 1993
反应条件
potassium carbonate in dimethyl sulfoxide
参考文献
Klunk, William E.; Mathis JR., Chester A.; Wang, Yanming
Patent: US2002/133019 A1, 2002 ;
反应条件
1: 4-iodo-N,N-dimethylaniline With lithium chloride; zinc
Inert atmosphere;
2: 2-(methylthio)benzothiazole With bis(acetylacetonate)nickel(II); bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran
T=25°C; Inert atmosphere;
参考文献
Metzger, Albrecht; Melzig, Laurin; Knochel, Paul
Synthesis, 2010 , # 16 art. no. T10210SS, p. 2853 - 2858
反应条件
1: 2-(methylthio)benzothiazole With bis(acetylacetonate)nickel(II); bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran
0.166667 h; Inert atmosphere;
2: C8H10INZn*ClLi in tetrahydrofuran
T=25°C; 5 h; Inert atmosphere;
参考文献
Melzig, Laurin; Metzger, Albrecht; Knochel, Paul
Chemistry - A European Journal, 2011 , vol. 17, # 10 p. 2948 - 2956
