反应条件
1: sodium azide / methanol; H2O / 1.5 h / Heating 2: conc. hydrochlorid acid, H2 / 10 percent palladium-charcoal / ethanol 3: 80 percent / ethanol; H2O 4: 72 percent / triethylamine, / ethanol / 16 h / Heating 5: 79 percent / 2M hydrochloric acid / H2O / 0.5 h / Heating 6: 76 percent / sodium dithionite / aq. NaOH / Heating View Scheme
参考文献
Al-Hassan, Saiba S.; Cameron, Robert J.; Curran, Adrian W. C.; Lyall, William J. S.; Nicholson, Sydney H.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1645 - 1660