2-甲基-4-甲氧基苯胺合成路线 (共 58 条)
反应条件
hydrogen; platinum(IV) oxide in isopropyl alcohol P=2327.2 Torr;
参考文献
Young, David C.; Vouros, Paul; Holick, Michael F.; Higuchi, Tetsuo
Analytical Chemistry, 1992 , vol. 64, # 8 p. 837 - 842
反应条件
ammonium hydroxide; copper(l) iodide; potassium carbonate; (2S,4R)-2-carboxy-4-hydroxypyrrolidine in dimethyl sulfoxide T=70°C; 36 h;
参考文献
Jiang, Liqin; Lu, Xu; Zhang, Hui; Jiang, Yongwen; Ma, Dawei
Journal of Organic Chemistry, 2009 , vol. 74, # 12 p. 4542 - 4546
反应条件
[Pd(η3-1-Ph-allyl)(μ-Cl)]2; (Mor-DalPhos); ammonia; sodium t-butanolate in 1,4-dioxane T=65°C; 24 h; Inert atmosphere; chemoselective reaction;
参考文献
Lundgren, Rylan J.; Peters, Brendan D.; Alsabeh, Pamela G.; Stradiotto, Mark
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4071 - 4074
反应条件
acetic acid; zinc 0.75 h; Ambient temperature;
参考文献
Mitchell, Helen; Leblanc, Yves
Journal of Organic Chemistry, 1994 , vol. 59, # 3 p. 682 - 687
反应条件
1: potassium carbonate; xylene 2: tin (II)-chloride; hydrochloric acid View Scheme
参考文献
Journal of the Chemical Society, , vol. 123, p. 2989
Journal of the Chemical Society, , vol. 125, p. 1305
参考文献
Journal of the American Chemical Society, , vol. 41, p. 1457
反应条件
1: alkali 2: hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 41, p. 1457
反应条件
1: 92 percent / ZnCl2 / diethyl ether; CH2Cl2 / 0.5 h / 25 °C 2: 76 percent / Zn, glacial acetic acid / 0.75 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 59, # 3 p. 682 - 687
反应条件
1: HNO3, AcOH 2: (methylation) 3: N2H4*H2O / Raney-Ni View Scheme
参考文献
Tetrahedron, , vol. 34, p. 3611 - 3615
反应条件
lithium aluminium tetrahydride; palladium on activated charcoal 1) THF, 20 min, -30 deg C, 2) 20 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 43, # 18 p. 4221 - 4226