3,3-二乙基氧杂环丁烷合成路线 （共 10 条）
反应条件
sodium hydride in tetrahydrofuran; mineral oil T=0 - 20°C; 73 h;
参考文献
Rix, Diane; Ballesteros-Garrido, Rafael; Zeghida, Walid; Besnard, Celine; Lacour, Jerome
Angewandte Chemie - International Edition, 2011 , vol. 50, # 32 p. 7308 - 7311
反应条件
potassium hydroxide T=100°C;
参考文献
Searles et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 1839,1842
反应条件
1: acetic acid; water; hydrobromic acid / anschliessendes Erhitzen mit Bromwasserstoff in Essigsaeure und Erwaermen des Reaktionsprodukts mit Aethanol unter Zusatz von wss.Bromwasserstoffsaeure 2: aqueous KOH-solution View Scheme
参考文献
Rix, Diane; Ballesteros-Garrido, Rafael; Zeghida, Walid; Besnard, Celine; Lacour, Jerome
Angewandte Chemie - International Edition, 2011 , vol. 50, # 32 p. 7308 - 7311
反应条件
decompn. at 200°C (0.5 h);
参考文献
Gmelin Handbook: Sn: Org.Comp.12, 1.4.1.1.1.5.2.1.7, page 69 - 97
参考文献
Delmond,B. et al.
Journal of Organometallic Chemistry, 1973 , vol. 47, p. 337 - 350
反应条件
potassium cyanide; water T=320°C; pyrolysis, var. reag.: LiCl, KOH;
参考文献
Bartok, M.; Molnar, A.; Bartok-Bozoki, G.
Acta Chimica Hungarica, 1983 , vol. 114, # 3-4 p. 375 - 380
反应条件
water; lithium chloride T=320°C; pyrolysis, var. reag.: KOH, KCN;
参考文献
Bartok, M.; Molnar, A.; Bartok-Bozoki, G.
Acta Chimica Hungarica, 1983 , vol. 114, # 3-4 p. 375 - 380
反应条件
water; lithium chloride T=320°C; pyrolysis, var. reag.: KOH, KCN; var. conc. of reag.; Product distribution;
参考文献
Bartok, M.; Molnar, A.; Bartok-Bozoki, G.
Acta Chimica Hungarica, 1983 , vol. 114, # 3-4 p. 375 - 380
反应条件
water; water-d2 multistep reaction; 1) pentane, 25 deg C, 4 h; Product distribution;
参考文献
Tetrahedron Letters, , vol. 28, # 46 p. 5747 - 5750
参考文献
Searles et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 948,950
