3-氯-5-甲基硫代-1,2,4-噻二唑合成路线 (共 2 条)
反应条件
sulfuryl dichloride in chloroform 3.5 h; Heating;
参考文献
Wittenbrook,L.S. et al.
Journal of Organic Chemistry, 1973 , vol. 38, # 3 p. 465 - 471
反应条件
tetraethylammonium bromide 1.) CH3CN, electrolysis by 1.6 V (against SCE) with Pt cathode, Ag anode, 2.) 2 h, room temp.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Ruettinger, H.-H.; Walek, W.; Matschiner, H.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 5 p. 823 - 828