2-(4-氯苯基)苯并咪唑合成路线 (共 69 条)
反应条件
boric acid; glycerol in water T=80°C;
参考文献
Australian Journal of Chemistry, , vol. 62, # 2 p. 140 - 144
反应条件
in water T=120°C; 16 h; Sealed tube;
参考文献
RSC Advances, , vol. 4, # 8 p. 3768 - 3773
参考文献
Tetrahedron, , vol. 50, # 8 p. 2485 - 2496
反应条件
1: 76 percent Chromat. / 3 Angstroem molecular sieves; DBU; carbon monoxide / Se / dioxane / 3 h / 120 °C / 22800 Torr View Scheme
参考文献
Synlett, , # 1 art. no. U26605ST, p. 109 - 111
反应条件
1: 76 percent Chromat. / 3 Angstroem molecular sieves; DBU; carbon monoxide / Se / dioxane / 3 h / 120 °C / 22800 Torr View Scheme
参考文献
Synlett, , # 1 art. no. U26605ST, p. 109 - 111
反应条件
1: 4-chloro-aniline With hydrogenchloride; sodium nitrite in water Cooling; 2: 1H-benzo[d]imidazole With sodium acetate in water T=20°C; 51 h; Cooling;
参考文献
European Journal of Medicinal Chemistry, , vol. 44, # 3 p. 1119 - 1127
反应条件
1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate T=160°C; 0.25 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 53, # 19 p. 2440 - 2443
反应条件
T=250°C; P=0.045 Torr; 0.25 h; Pyrolysis;
参考文献
Journal of Heterocyclic Chemistry, , vol. 45, # 3 p. 723 - 727
反应条件
carbon monoxide in toluene byproducts: CO2; High Pressure; (N2), autoclave; CO is introduced (P(CO)=50 bar), react. of Ru3(CO)12 with ClC6H4CHNC6H4NO2 at 220°C for 3.5 h under magnetic stirring; autoclave is cooled rapidly (ice bath) and then blown off, substituted benzimidazole is filtered off, Ru complex isolated by chromy. (silica gel, CH2Cl2/EtOH);
参考文献
Journal of Molecular Catalysis, , vol. 72, p. 283 - 298
参考文献
Chemistry Letters, , p. 1117 - 1118